Hydrazine → 4-(Morpholin-4-yl)butan-1-amine

HRID 1463798

반응식

HRID 1463798 반응식
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][NH2:1])[CH2:4][CH2:5][O:6][CH2:7][CH2:8]1

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 220025214-Morpholinylbutylphthalimide

생성물 1

HCID 2336114-(Morpholin-4-yl)butan-1-amine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 4-morpholinylbutylphthalimide (231 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

후처리

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

출처 및 근거

ORD 기록
ord-d4eac5790f2e4025960d08d0b535aae2
출처 데이터셋
uspto-grants-1994_04
특허 번호
US05302593

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