Hydrazine → 8-Morpholinooctylamine

HRID 1463808노트

반응식

HRID 1463808 반응식
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH2:1])[CH2:4][CH2:5][O:6][CH2:7][CH2:8]1

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 537680558-Morpholinyloctylphthalimide

생성물 1

HCID 222376608-Morpholinooctylamine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-morpholinyloctylphthalimide (275 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

후처리

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

출처 및 근거

ORD 기록
ord-ebb45c81766146a59970e0a408d0868a
출처 데이터셋
uspto-grants-1994_04
특허 번호
US05302593

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