Hydrazine → HCID 54275604, 화합물

HRID 1463817노트

반응식

HRID 1463817 반응식
[NH2:1]N.[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13]C1C=CC=C2C(NC(=O)C=12)=O>CO>[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13][NH2:1]

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 538263884-(N-methylpiperazinyl)butylphthalimide

생성물 1

HCID 54275604HCID 54275604, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 4-(N-methylpiperazinyl)butylphthalimide (240 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

후처리

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

출처 및 근거

ORD 기록
ord-8fe237a629f34fea9a2a27849c8afeba
출처 데이터셋
uspto-grants-1994_04
특허 번호
US05302593

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