Hydrazine → 8-Pyrrolidinyloctylamine

HRID 1463822노트

반응식

HRID 1463822 반응식
[NH2:1]N.[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:7][CH2:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7]1

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 542934218-Pyrrolidinyloctylphthalimide

생성물 1

HCID 199335008-Pyrrolidinyloctylamine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-pyrrolidinyloctylphthalimide (263 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

후처리

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

출처 및 근거

ORD 기록
ord-8b4d10a573ec41db9f7b3f9c763bc267
출처 데이터셋
uspto-grants-1994_04
특허 번호
US05302593

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