Hydrazine → 8-Piperidinyloctylamine

HRID 1463824노트

반응식

HRID 1463824 반응식
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]1

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 540305088-Piperidinyloctylphthalimide

생성물 1

HCID 110092698-Piperidinyloctylamine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-piperidinyloctylphthalimide (274 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

후처리

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

출처 및 근거

ORD 기록
ord-7b07b0fd85c84a33a3b59b3d7d5fd1eb
출처 데이터셋
uspto-grants-1994_04
특허 번호
US05302593

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