Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylcyanamide → HCID 178466076, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylcyanamide | HCID 15112 | — |
| 반응물 | 4'-Acetyl-2-aminobiphenyl hydrochloride | HCID 19089305 | — |
| 용매 | M-Cresol | HCID 342 | — |
| 생성물 | HCID 178466076 | HCID 178466076 | — |
반응 단계
Reaction of dry 4'-acetyl-2-aminobiphenyl hydrochloride (2.6 g) with N,N-dimethylcyanamide (2.5 ml) in m-cresol (7 ml) at 80° C. for 5 hours gave N-(4'-acetyl-2-biphenylyl)-N',N'-dimethylguanidine (2.3 g) as a colourless solid (m.p. 174°-175° C.) which was recrystallised from a mixture of acetone and hexane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05302720 |
| 출처 데이터셋 | uspto-grants-1994_04 |
| ORD ID | ord-c9fa1c6364584361998827a21eb5086a |
| 출처 메모 | uspto-grants-1994_04 |