Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thiophosgene → 5-Fluoro-2-biphenylylisothiocyanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thiophosgene | HCID 10040 | — |
| 반응물 | 4-Fluoro-2-phenylaniline | HCID 19089219 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 5-Fluoro-2-biphenylylisothiocyanate | HCID 19089275 | — |
반응 단계
Reaction of 2-amino-5-fluorobiphenyl (7.8 g) with thiophosgene (7.2 g) in a mixture of dioxan (15 ml) and water (60 ml) at ambient temperature for 2 hours yielded 5-fluoro-2-biphenylylisothiocyanate as a brown oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05302720 |
| 출처 데이터셋 | uspto-grants-1994_04 |
| ORD ID | ord-e1352bff720d49a485c8be120371db65 |
| 출처 메모 | uspto-grants-1994_04 |