Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methylthiophene → 3-Methylthiophene-2-sulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methylthiophene | HCID 12024 | — |
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 반응물 | Chlorosulfonic acid | HCID 24638 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 3-Methylthiophene-2-sulfonamide | HCID 341083 | — |
반응 단계
The procedure of Example 3A was followed with 3-methylthiophene (10.0 g, 102 mmole), chlorosulfonic acid (29.58 g, 255 mmoles) in chloroform (200 ml), concentrated ammonium hydroxide, to provide 3-methyl-2-thiophenesulfonamide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05302724 |
| 출처 데이터셋 | uspto-grants-1994_04 |
| ORD ID | ord-5c67b8fc142f4e7480be130afff425bf |
| 출처 메모 | uspto-grants-1994_04 |