Methanol → HCID 11747608, 화합물

HRID 1464142노트

반응식

HRID 1464142 반응식
[CH3:1][Si:2]([CH3:13])([CH2:4][Si:5](Cl)([Cl:11])[CH2:6][Si:7]([CH3:10])([CH3:9])[CH3:8])[CH3:3].[CH3:14][OH:15]>>[CH3:1][Si:2]([CH3:13])([CH2:4][Si:5]([Cl:11])([O:15][CH3:14])[CH2:6][Si:7]([CH3:10])([CH3:9])[CH3:8])[CH3:3]

참가 물질

3

반응물 2

HCID 887MethanolHCID 11747735Bis(trimethylsilylmethyl)dichlorosilane

생성물 1

HCID 11747608HCID 11747608, 화합물수율 74%

반응 조건

온도
70 °C

실험 절차

13.7 g(50 mmoles) of 2,2,6,6-tetramethyl-4,4-dichloro-2,4,6-trisilaheptane were placed in the flask of the same set as Example 1, and then 1.8 g(60 mmoles) of dry methanol were added. The mixture was heated at 70° C. for 2 hrs. The amount of the product was 9.92 g and the yield 74%.

출처 및 근거

ORD 기록
ord-b6efa47268994222961eb742258b7bf6
출처 데이터셋
uspto-grants-1994_04
특허 번호
US05302734

반응 노트

불러오는 중…