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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1464209생성일: 2026년 10월 26일

Acetic Anhydride → (S)-Benzyl (tetrahydro-2,5-dioxo-3-furyl)carbamate

https://huagongshe.com/reaction/1464209

반응식

참여 물질

역할이름HCID투입량
반응물Acetic AnhydrideHCID 7918—
반응물N-(Benzyloxycarbonyl)aspartic acidHCID 2723942—
용매Acetic AcidHCID 176—
생성물(S)-Benzyl (tetrahydro-2,5-dioxo-3-furyl)carbamateHCID 11128682—

반응 단계

For example, N-benzyloxycarbonyl-L-aspartic acid is dissolved in a large excess of acetic anhydride, the acetic acid formed by the reaction and the excess acetic anhydride are distilled off under reduced pressure and the effect of any acetic acid remaining in the residue is removed by the addition of an organic solvent to give N-benzyloxycarbonyl-L-aspartic anhydride [J. Am. Chem. Soc., 81, 167-173 (1959)].

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05302743
출처 데이터셋uspto-grants-1994_04
ORD IDord-0d00a997b1df4e23a14cef71c9b78832
출처 메모uspto-grants-1994_04