Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → (S)-Benzyl (tetrahydro-2,5-dioxo-3-furyl)carbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | N-(Benzyloxycarbonyl)aspartic acid | HCID 2723942 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | (S)-Benzyl (tetrahydro-2,5-dioxo-3-furyl)carbamate | HCID 11128682 | — |
반응 단계
For example, N-benzyloxycarbonyl-L-aspartic acid is dissolved in a large excess of acetic anhydride, the acetic acid formed by the reaction and the excess acetic anhydride are distilled off under reduced pressure and the effect of any acetic acid remaining in the residue is removed by the addition of an organic solvent to give N-benzyloxycarbonyl-L-aspartic anhydride [J. Am. Chem. Soc., 81, 167-173 (1959)].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05302743 |
| 출처 데이터셋 | uspto-grants-1994_04 |
| ORD ID | ord-0d00a997b1df4e23a14cef71c9b78832 |
| 출처 메모 | uspto-grants-1994_04 |