Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isoamyl Nitrite → 2-Methyl-4-nitrosoresorcinol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isoamyl Nitrite | HCID 8053 | — |
| 반응물 | 2-Methylresorcinol | HCID 11843 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Methyl-4-nitrosoresorcinol | HCID 100616 | — |
반응 단계
19.8 g. 2-Methylresorcinol and 13.4 g. potassium hydroxide are dissolved in 120 ml. ethanol and cooled to 5° C. 24 ml. Isopentyl nitrite are added dropwise thereto, the reaction mixture is stirred for 3 hours and the precipitate is filtered off with suction. The yellow solid material is stirred into 200 ml. 5N sulphuric acid, the bright yellow product thereby precipitating out. Yield 22 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05304645 |
| 출처 데이터셋 | uspto-grants-1994_04 |
| ORD ID | ord-63c2a46ced484bca92e3fbc8bb0f2b1c |
| 출처 메모 | uspto-grants-1994_04 |