Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → 2-Nitro-5-(4-acetylamino-1-piperidyl)benzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Formaldehyde | HCID 712 | — |
| 반응물 | 2-Nitro-5-(4-acetylamino-1-piperidyl)benzaldehyde dimethylacetal | HCID 19086863 | — |
| 촉매 | Hydrochloric Acid | HCID 313 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Nitro-5-(4-acetylamino-1-piperidyl)benzaldehyde | HCID 19086846 | — |
반응 단계
0.3 Gram of 2-nitro-5-(4-acetylamino-1-piperidyl)benzaldehyde dimethylacetal, 5 ml of formalin, 1 ml of ethanol and 2 drops of concentrated hydrochloric acid were refluxed by heating. After the reaction was completed, the solvent was removed by evaporation to obtain the residue, then water was added to the residue. The crystals formed were collected by filtration to yield 0.22 g of 2-nitro-5-(4-acetylamino-1-piperidyl)benzaldehyde.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05306719 |
| 출처 데이터셋 | uspto-grants-1994_04 |
| ORD ID | ord-24500cb7809f4f38bdc83cb7fb68bc53 |
| 출처 메모 | uspto-grants-1994_04 |