Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrofluoric Acid → 2-Fluoro-m-xylene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrofluoric Acid | HCID 14917 | — |
| 반응물 | 2,6-Dimethylphenyl carbonochloridate | HCID 271618 | — |
| 생성물 | 2-Fluoro-m-xylene | HCID 123065 | 51% |
반응 단계
1000 ml of anhydrous hydrogen fluoride were placed at 0° C. in a stainless steel laboratory autoclave and 500 g of 2,6-dimethylphenyl chloroformate were added dropwise. The reaction was carried out and the reaction mixture worked up as described in Example 9. 2,6-Dimethylfluorobenzene was obtained in a yield of 51%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05306849 |
| 출처 데이터셋 | uspto-grants-1994_04 |
| ORD ID | ord-815b8636b4344f7db94ab8dea359cbc5 |
| 출처 메모 | uspto-grants-1994_04 |