Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 2-(4-bromophenoxy)acetate → 2-(4-Bromophenoxy)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 2-(4-bromophenoxy)acetate | HCID 248825 | — |
| 반응물 | Ammonia methanol | HCID 21705897 | — |
| 생성물 | 2-(4-Bromophenoxy)acetamide | HCID 302864 | 98% |
반응 단계
7M-Ammonia methanol solution (10 ml, 70 mmol) was added to ethyl 2-(4-bromophenoxy)acetate (1.0 g, 3.86 mmol), and the mixture was stirred at room temperature for 2.5 hrs. The reaction mixture was concentrated under reduced pressure to give 2-(4-bromophenoxy)acetamide (870 mg, yield 98%) as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08999989B2 |
| 출처 데이터셋 | uspto-grants-2015_04 |
| ORD ID | ord-0474a42cf25b40b6b4b1e58b784d031d |
| 출처 메모 | uspto-grants-2015_04 |