Acetylene → 5,5'-(1,2-Ethynediyl)bis-(1,3-Isobenzofurandione)

반응식

Br[C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[C:7](=[O:11])[O:6][C:5]2=[O:12].[CH:13]#[CH:14]>>[C:13]([C:10]1[CH:9]=[C:8]2[C:4](=[CH:3][CH:2]=1)[C:5](=[O:12])[O:6][C:7]2=[O:11])#[C:14][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[C:7](=[O:11])[O:6][C:5]2=[O:12]

참가 물질

반응물 2

HCID 6326Acetylene

HCID 665904-Bromophthalic anhydride

생성물 1

HCID 589864785,5'-(1,2-Ethynediyl)bis-(1,3-Isobenzofurandione)

실험 절차

According to an aspect of the invention, a 5-haloisobenzofuran-1,3-dione, such as 5-bromoisobenzofuran-1,3-dione, is reacted with ethyne to obtain 5,5′-(ethyne-1,2-diyl)bis(isobenzofuran-1,3-dione).

출처 및 근거

ORD 기록: ord-32ee3d4e9b4a4fdca6f9186eb948dfb5
출처 데이터셋: uspto-grants-2015_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09018401B2

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