Hydroxylamine → HCID 43248107, 화합물

HRID 1476672노트

반응식

HRID 1476672 반응식
[CH2:1]([O:4][CH2:5][C:6]#[N:7])[CH2:2][CH3:3].[NH2:8][OH:9]>C(Cl)Cl>[OH:9]/[N:8]=[C:6](\[NH2:7])/[CH2:5][O:4][CH2:1][CH2:2][CH3:3]

참가 물질

4

반응물 2

HCID 787HydroxylamineHCID 189809232-Propoxyacetonitrile

생성물 1

HCID 43248107HCID 43248107, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

반응 조건

온도
100 °C

실험 절차

A mixture of propoxyacetonitrile (3.03 g) and hydroxylamine (2.01 g, 50 wt % in water) is stirred for 2 h at 100° C. At RT DCM is added, the organic phase is separated, dried over sodium sulfate and concentrated under reduced pressure to give the title compound as an oil.

후처리

  1. customthe organic phase is separated
  2. dry with materialdried over sodium sulfate
  3. concentrationconcentrated under reduced pressure

출처 및 근거

ORD 기록
ord-1489afd5ce5c4c1e95fdd821af9fbff7
출처 데이터셋
uspto-grants-2015_04
특허 번호
US09018175B2

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