Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfuric Acid → 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide sulfate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide | HCID 71811587 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide sulfate | HCID 118387004 | 72% |
반응 단계
2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide dissolved in EA, stirred at room temperature, while dropped H2SO4 into mixture till occurred to white solid. The reaction mixture was filtered to get White solid; 72% yield;
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09402819B2 |
| 출처 데이터셋 | uspto-grants-2016_08 |
| ORD ID | ord-46c5fcb07c94481a8e8f0d3a8d9e85a9 |
| 출처 메모 | uspto-grants-2016_08 |