Cyclobutanone → HCID 90203774, 화합물

HRID 1480192노트

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HRID 1480192 반응식
Br[C:2]1[C:3]([Cl:9])=[CH:4][C:5]([Cl:8])=[N:6][CH:7]=1.[C:10]1(=[O:14])[CH2:13][CH2:12][CH2:11]1>>[Cl:9][C:3]1[CH:4]=[C:5]([Cl:8])[N:6]=[CH:7][C:2]=1[C:10]1([OH:14])[CH2:13][CH2:12][CH2:11]1

참가 물질

3

반응물 2

HCID 14496CyclobutanoneHCID 121751335-bromo-2,4-dichloropyridine

생성물 1

HCID 90203774HCID 90203774, 화합물

실험 절차

The title compound was synthesized in analogy to Example 123a, using 5-bromo-2,4-dichloropyridine (CAN 849937-96-8) and cyclobutanone (CAN 1191-95-3) as starting materials and isolated (5.1 g, 76%); MS (ESI, m/z): 218.4 (M+H+).

후처리

  1. customisolated (5.1 g, 76%)

출처 및 근거

ORD 기록
ord-de8d8d33620a439096a33881ce204152
출처 데이터셋
uspto-grants-2016_08
특허 번호
US09409866B2

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