Resorcinol → HCID 86680722, 화합물

HRID 1483233

반응식

HRID 1483233 반응식
[CH:1]([C:3]1[CH:16]=[CH:15][C:6]([O:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([OH:14])=[O:13])=[CH:5][CH:4]=1)=O.[C:17]1([CH:24]=[CH:23][CH:22]=[C:20]([OH:21])[CH:19]=1)[OH:18].C(N1[C:36]2[C:31](=[CH:32][CH:33]=[C:34]([OH:37])[CH:35]=2)C(C)=CC1(C)C)C.C(C1C=CC(OCC(O)=O)=CC=1)=O>CO>[OH:18][C:17]1[CH:24]=[CH:23][C:22]2[C:1]([C:3]3[CH:16]=[CH:15][C:6]([O:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([OH:14])=[O:13])=[CH:5][CH:4]=3)=[C:31]3[C:36]([O:21][C:20]=2[CH:19]=1)=[CH:35][C:34](=[O:37])[CH:33]=[CH:32]3

참가 물질

6

반응물 4

HCID 5054ResorcinolHCID 89177Acetic acid, 2-(4-formylphenoxy)-HCID 154511031-Ethyl-2,2,4-trimethyl-1,2-dihydroquinolin-7-olHCID 214628695-(4-Formylphenoxy)pentanoic acid

생성물 1

HCID 86680722HCID 86680722, 화합물수율 26%

시약·촉매·용매 1

HCID 887Methanol용매2회

실험 절차

Dye 9 (shown below) was prepared using the procedure described in Example 4 except that 5-(4-formylphenoxy)pentanoic acid and resorcinol substituted for 1-ethyl-2,2,4-trimethyl-1,2-dihydroquinolin-7-ol and 2-(4-formylphenoxy)acetic acid. Yield: 26%. λabs=486 nm (in methanol), λem=513 nm (in methanol).

후처리

  1. customDye 9 (shown below) was prepared

출처 및 근거

ORD 기록
ord-e2fd008cb4de45bd94b5b3f8cdf17393
출처 데이터셋
uspto-grants-2016_08
특허 번호
US09416153B2

연결된 노트

불러오는 중…