Ethanol → L-Carnitine Vinpocetine

HRID 1484008

반응식

HRID 1484008 반응식
[OH:1][C@H:2]([CH2:8][C:9](=[O:11])[O-:10])[CH2:3][N+:4]([CH3:7])([CH3:6])[CH3:5].[CH3:12][CH2:13][C@:14]12[CH:30]=[C:29]([C:31]([O:33][CH2:34][CH3:35])=[O:32])[N:28]3[C:20]4=[C:21]([CH2:36][CH2:37][N:18]([C@@H:19]14)[CH2:17][CH2:16][CH2:15]2)[C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][C:27]=13.C(O)C.C(OC(C1C=CC(O)=CC=1)=O)C>OCC(CO)O>[CH3:12][CH2:13][C@:14]12[CH:30]=[C:29]([C:31]([O:33][CH2:34][CH3:35])=[O:32])[N:28]3[C:20]4=[C:21]([CH2:36][CH2:37][N:18]([C@@H:19]14)[CH2:17][CH2:16][CH2:15]2)[C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][C:27]=13.[OH:1][C@H:2]([CH2:8][C:9](=[O:10])[O-:11])[CH2:3][N+:4]([CH3:7])([CH3:5])[CH3:6]

참가 물질

6

반응물 4

HCID 702EthanolHCID 8434EthylparabenHCID 10917(-)-CarnitineHCID 443955Vinpocetine

생성물 1

HCID 86298728L-Carnitine Vinpocetine

시약·촉매·용매 1

HCID 753Glycerol용매

반응 조건

온도
55 °C

실험 절차

Process: Take L-carnitine and vinpocetine, add into ethanol and boil to completely dissolution, add ethylparaben and stir, and add defined amount of glycerin and stir uniformly, and then slowly add the solution into glycerinated gelatin substrate to preserve heat for later use. Add polysorbate and stir uniformly, and then slowly stir the solution and add into the said glycerinated gelatin substrate, stir well and preserve the heat at 55° C., and affuse into the membrane, and cool them down.

후처리

  1. dissolutionboil to completely dissolution
  2. additionadd
  3. stirringstir uniformly
  4. additionslowly add the solution
  5. temperatureto preserve heat for later use
  6. stirringslowly stir the solution
  7. additionadd into the
  8. stirringstir well
  9. temperaturecool them down

출처 및 근거

ORD 기록
ord-6ec5712844be46cdb9bde30eea2ff6f8
출처 데이터셋
uspto-grants-2016_08
특허 번호
US09421181B2

연결된 노트

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