Ethanol → L-Carnitine Vinpocetine

HRID 1484009

반응식

HRID 1484009 반응식
[OH:1][C@H:2]([CH2:8][C:9](=[O:11])[O-:10])[CH2:3][N+:4]([CH3:7])([CH3:6])[CH3:5].[CH3:12][CH2:13][C@:14]12[CH:30]=[C:29]([C:31]([O:33][CH2:34][CH3:35])=[O:32])[N:28]3[C:20]4=[C:21]([CH2:36][CH2:37][N:18]([C@@H:19]14)[CH2:17][CH2:16][CH2:15]2)[C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][C:27]=13.C(O)C.C(OC(C1C=CC(O)=CC=1)=O)C>OCC(CO)O>[OH:1][C@H:2]([CH2:8][C:9](=[O:10])[O-:11])[CH2:3][N+:4]([CH3:7])([CH3:5])[CH3:6].[CH3:12][CH2:13][C@:14]12[CH:30]=[C:29]([C:31]([O:33][CH2:34][CH3:35])=[O:32])[N:28]3[C:20]4=[C:21]([CH2:36][CH2:37][N:18]([C@@H:19]14)[CH2:17][CH2:16][CH2:15]2)[C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][C:27]=13

참가 물질

6

반응물 4

HCID 702EthanolHCID 8434EthylparabenHCID 10917(-)-CarnitineHCID 443955Vinpocetine

생성물 1

HCID 86298728L-Carnitine Vinpocetine

시약·촉매·용매 1

HCID 753Glycerol용매

반응 조건

온도
55 °C

실험 절차

Process: Take L-carnitine and vinpocetine, add into ethanol and boil to completely dissolution, add ethylparaben and stir, and add defined amount of glycerin and stir uniformly, and then slowly add the solution into glycerinated gelatin substrate to preserve heat for later use. Add polysorbate and stir uniformly, and then slowly stir the solution and add it into the said glycerinated gelatin substrate, stir well and preserve the heat at 55° C., and affuse into the membrane, and cool them down.

후처리

  1. dissolutionboil to completely dissolution
  2. additionadd
  3. stirringstir uniformly
  4. additionslowly add the solution
  5. temperatureto preserve heat for later use
  6. stirringslowly stir the solution
  7. additionadd it into the
  8. stirringstir well
  9. temperaturecool them down

출처 및 근거

ORD 기록
ord-0d90cf60a49f4759bb6288e96dc232f1
출처 데이터셋
uspto-grants-2016_08
특허 번호
US09421181B2

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