1-Bromo-4-nitrobenzene → 1-[8-(Cyclohexylmethoxy)octyl]-4-nitrobenzene

반응식

[CH2:1]([O:9][CH2:10][CH:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH:7]=[CH2:8].Br[C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1>>[CH:11]1([CH2:10][O:9][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:18]2[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=2)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]1

참가 물질

반응물 2

HCID 114661-Bromo-4-nitrobenzene

HCID 53248071HCID 53248071, 화합물

생성물 1

HCID 532481341-[8-(Cyclohexylmethoxy)octyl]-4-nitrobenzene수율 48%

실험 절차

General procedure M was used to convert 4.56 mmol of 11c and 5.02 mmol of 1-bromo-4-nitrobenzene to 2.19 mmol (48%) of the title compound.

출처 및 근거

ORD 기록: ord-01e8a4ddc11f4708b2ed5c0c173e25d4
출처 데이터셋: uspto-grants-2016_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09421177B2

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