Ammonia → 3-Amino-1,2,4-triazine mesylate

HRID 1484496노트

반응식

HRID 1484496 반응식
C(OC1C=C(C=[CH:17][CH:18]=1)C(OC)=O)C1C=CC=CC=1.[S:19]([OH:23])(=[O:22])(=[O:21])[CH3:20].S(O)(=O)(=O)C.[NH2:29][NH:30][C:31]([NH2:33])=[NH:32].N>>[S:19]([OH:23])(=[O:22])(=[O:21])[CH3:20].[NH2:33][C:31]1[N:30]=[N:29][CH:17]=[CH:18][N:32]=1

참가 물질

4

반응물 3

HCID 222AmmoniaHCID 13368031Methyl 3-(benzyloxy)benzoateHCID 178505340HCID 178505340, 화합물

생성물 1

HCID 866497313-Amino-1,2,4-triazine mesylate

실험 절차

Prepared by reacting acenaphthenequinone (3) with aminoguanidine bismesylate for 24 hrs using the above procedure except that the basification step with ammonia was omitted. The title compound was obtained as bright yellow prisms in 83.2%, mpt=264-266° (froth)

후처리

  1. customPrepared
  2. customfor 24 hrs

출처 및 근거

ORD 기록
ord-a8de5f0905094df09005f1c293579976
출처 데이터셋
uspto-grants-2016_08
특허 번호
US09422253B2

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