3-Phenylcyclobutanone → HCID 178521034, 화합물

반응식

C1(C2C[C:9](=[O:11])C2)C=CC=CC=1.[F:12][C:13]1[CH:18]=[CH:17][C:16]([CH:19]2[CH2:22][C:21](=O)[CH2:20]2)=[CH:15][CH:14]=1>>[F:12][C:13]1[CH:18]=[CH:17][C:16]([C@H:19]2[CH2:22][C@H:21]([CH:9]=[O:11])[CH2:20]2)=[CH:15][CH:14]=1

참가 물질

반응물 2

HCID 1429633-Phenylcyclobutanone

HCID 114125713-(4-Fluorophenyl)cyclobutan-1-one

생성물 1

HCID 178521034HCID 178521034, 화합물

실험 절차

Instead of 3-phenylcyclobutanone, 3-(4-fluorophenyl)cyclobutanone (4.63 g) was used and treated by the same technique as in Reference Example 24-1 to give the titled compound as a colorless oil (720 mg).

후처리

additiontreated by the same technique as in Reference Example 24-1

출처 및 근거

ORD 기록: ord-57799256a8154451952fcaf7affda71a
출처 데이터셋: uspto-grants-2016_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09422240B2

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