N,N-Diethyl-beta-oxobenzenepropanamide → Dioxomolybdenum(VI) bis(N,N-diethyl-3-phenyl-3-oxopropane amidate)

HRID 1485916노트

반응식

HRID 1485916 반응식
O.O.[O-:3][Mo:4]([O-])(=O)=[O:5].[Na+].[Na+].[CH2:10]([N:12]([CH2:24][CH3:25])[C:13](=[O:23])[CH2:14][C:15]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[O:16])[CH3:11]>>[CH2:24]([N:12]([CH2:10][CH3:11])[C:13](=[O:23])[CH2:14][C:15]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[O:16])[CH3:25].[CH2:24]([N:12]([CH2:10][CH3:11])[C:13](=[O:23])[CH2:14][C:15]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[O:16])[CH3:25].[O:3]=[Mo+2:4]=[O:5]

참가 물질

3

반응물 2

HCID 12196321N,N-Diethyl-beta-oxobenzenepropanamideHCID 16211258Sodium molybdate dihydrate

생성물 1

HCID 131736770Dioxomolybdenum(VI) bis(N,N-diethyl-3-phenyl-3-oxopropane amidate)

실험 절차

2.05 g sodium molybdate dihydrate and 4.33 g N,N-diethyl-3-phenyl-3-oxopropanamide were reacted according to General Preparation Procedure B. The product consisted of 5.18 g of a yellow, microcrystalline solid.

후처리

  1. customaccording to General Preparation Procedure B

출처 및 근거

ORD 기록
ord-8a131ff279c648a1b8841c496e35c91a
출처 데이터셋
uspto-grants-2016_08
특허 번호
US09422390B2

반응 노트

불러오는 중…