참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 4,7-Methano-5H-inden-5-one, octahydro- | HCID 96509 | — |
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 용매 | Cyclohexane | HCID 8078 | — |
| 생성물 | 9-(4-Formylbenzylidene)-8-ketotricyclo[5.2.1.02,6]decane | HCID 54022151 | — |
반응 단계
A suspension of 40 mmol (6.3 g) of 8-ketotricyclo[5.2.1.02,6 ]decane and 60 mmol of sodium methoxide (11 g of a 30% solution) in 50 ml of cyclohexane are stirred at 50° C. for 30 minutes. 50 mmol (9.0 g) of terephthalaldehyde monodimethyl acetal are then added dropwise and the mixture is refluxed for 1 hour. It is then cooled to room temperature and 100 ml of water are added.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05677314 |
|---|
| 출처 데이터셋 | uspto-grants-1997_10 |
|---|
| ORD ID | ord-65eb37158b154bfcbc862fe249bc7eda |
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| 출처 메모 | uspto-grants-1997_10 |
|---|
