Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Imidazole → Diethyl 3-(tert-Butyldimethylsilyloxy)glutarate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Imidazole | HCID 795 | — |
| 반응물 | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| 반응물 | Diethyl 3-hydroxyglutarate | HCID 96259 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Diethyl 3-(tert-Butyldimethylsilyloxy)glutarate | HCID 13327289 | — |
반응 단계
Imidazole and tert-butylchlorodimethylsilane are added to a solution of diethyl 3-hydroxyglutarate in methylene chloride, and the reaction is performed to give diethyl 3-[(tert-butydimethylsilyl)oxy]pentanedioate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05677455 |
| 출처 데이터셋 | uspto-grants-1997_10 |
| ORD ID | ord-e4ee71123c4e460d8e6cc9a2a88f101a |
| 출처 메모 | uspto-grants-1997_10 |