참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methane | HCID 297 | — |
| 반응물 | 1-Bromooctadecane | HCID 8218 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Distearyl Ether | HCID 80526 | — |
반응 단계
Distearyl ether was synthesized by reacting stearyl bromide (Sigma) with PEG-900 in the presence of potassium hydroxide. Stearyl bromide (4.168 g in 10 ml toluene) was slowly added with stirring to 4.64 g of PEG-900 in 10 ml of toluene at 45° C. The mixture was then stirred at 60° C. for 30 min. and refluxed for 6 hrs. The final product was treated with charcoal, filtered and isolated from toluene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05681812 |
|---|
| 출처 데이터셋 | uspto-grants-1997_10 |
|---|
| ORD ID | ord-ff08e2589d3e43928ba24fb1c8f6c1c7 |
|---|
| 출처 메모 | uspto-grants-1997_10 |
|---|
