N,N-Dimethylaniline → N,N-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

HRID 1490479

반응식

HRID 1490479 반응식
CN(C)c1ccccc1>B1Oc2ccccc2O1.CC(C)(O)C(C)(C)O.CCN(CC)CC.c1ccc(B(c2ccccc2)c2ccccc2)cc1>CN(C)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1

참가 물질

6

반응물 1

HCID 949N,N-Dimethylaniline

생성물 1

HCID 2758659N,N-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline수율 88%

시약·촉매·용매 4

HCID 6425Pinacol시약HCID 8471Triethylamine시약HCID 67506Catecholborane시약HCID 70400Triphenylborane촉매

반응 조건

온도
100 °C

출처 및 근거

ORD 기록
ord-092f34ffbc8d4bf2834ae0e8a1b27f27
출처 데이터셋
Borylation dataset from Roche

연결된 노트

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