N,N-dihexylbenzamide → HCID 91820772, 화합물

HRID 1490829노트

반응식

HRID 1490829 반응식
CCCCCCN(CCCCCC)C(=O)c1ccccc1>C1=CCCC=CCC1.C1=CCCC=CCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1cccc(C)c1NC(=O)Nc1ccccc1-c1ccc(-c2ccccn2)nc1.[Ir].[Ir]>CCCCCCN(CCCCCC)C(=O)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1.CCCCCCN(CCCCCC)C(=O)c1cccc(B2OC(C)(C)C(C)(C)O2)c1

참가 물질

6

반응물 1

HCID 4577308N,N-dihexylbenzamide

생성물 2

HCID 91820772HCID 91820772, 화합물수율 25%HCID 140851879HCID 140851879, 화합물수율 7%

시약·촉매·용매 3

HCID 2733548Bis(pinacolato)diborane시약HCID 918207671-(2-([2,2'-Bipyridin]-5-yl)phenyl)-3-(2,6-dimethylphenyl)urea시약HCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridium촉매

반응 조건

온도
25 °C

출처 및 근거

ORD 기록
ord-3adba44b40f24be4a631ac45b3c80152
출처 데이터셋
Borylation dataset from Roche

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