Tert-butyl dibutylcarbamate → tert-butyl N-butyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl]carbamate

HRID 1490989

반응식

HRID 1490989 반응식
CCCCN(CCCC)C(=O)OC(C)(C)C>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCCCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc2ccc3cccnc3c2n1.[Ir].[Ir]>CCCCN(CCCCB1OC(C)(C)C(C)(C)O1)C(=O)OC(C)(C)C

참가 물질

6

반응물 1

HCID 56986891Tert-butyl dibutylcarbamate

생성물 1

HCID 162413303tert-butyl N-butyl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl]carbamate수율 49%

시약·촉매·용매 4

HCID 2733548Bis(pinacolato)diborane시약HCID 49133562-Methyl-1,10-phenanthroline시약HCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridium촉매HCID 9266Cyclooctane용매

반응 조건

온도
100 °C

출처 및 근거

ORD 기록
ord-c24db4f4c6ca4cdfa554aa01f0162a4c
출처 데이터셋
Borylation dataset from Roche

연결된 노트

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