N,3-dimethylbenzamide → N,5-dimethyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
반응식
CNC(=O)c1cccc(C)c1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCOC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].[Ir].[Ir].c1ccc(-c2ccccn2)nc1>CNC(=O)c1cc(C)ccc1B1OC(C)(C)C(C)(C)O1참가 물질
6
반응 조건
- 온도
- 60 °C
실험 절차
Isolated by chromatography using deactivated silica gel and ethyl acetate and petroleum ether (10:1 to 1:1) as the eluent.
출처 및 근거
- ORD 기록
- ord-954be7a85ca24616b1aac921066bbf62
- 출처 데이터셋
- Borylation dataset from Roche
반응 노트
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