참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Boric Acid | HCID 7628 | — |
| 반응물 | Hexylene Glycol | HCID 7870 | — |
| 용매 | Heptane | HCID 8900 | — |
| 생성물 | 4,4,6-Trimethyl-1,3,2-dioxaborinan-2-OL | HCID 352515 | — |
반응 단계
61.2 g of boric acid (1 mol) and 118.2 g of 2-methyl-2,4-pentanediol (1 mol) and 200 ml of heptane are charged to a reaction flask equipped with stirrer, Marcusson apparatus and reflux condenser. The reaction mixture is heated up to its reflux temperature (about 95° C.), with stirring, and is kept at that temperature for a 4-hour period.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05370807 |
|---|
| 출처 데이터셋 | uspto-grants-1994_12 |
|---|
| ORD ID | ord-eaeb699ad1e74e04bbf19442810f1b08 |
|---|
| 출처 메모 | uspto-grants-1994_12 |
|---|
