Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,5-Dichloro-3-nitrobenzoic acid → 2,5-Dichloro-3-nitrobenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,5-Dichloro-3-nitrobenzoic acid | HCID 6951 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | 2,5-Dichloro-3-nitrobenzoyl chloride | HCID 10106386 | 87.5% |
반응 단계
A mixture of 5.0 parts of 2,5-dichloro-3-nitrobenzoic acid and 16.2 parts of thionyl chloride was refluxed for 24 hours under argon. The reaction mixture was evaporated, yielding 4.74 parts (87.5%) of 2,5-dichloro-3-nitrobenzoyl chloride (interm. 66).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05371079 |
| 출처 데이터셋 | uspto-grants-1994_12 |
| ORD ID | ord-93a1812400df4f5a9a075dd26cbecb43 |
| 출처 메모 | uspto-grants-1994_12 |