Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Acetamide, N-(5-hydroxy-1-naphthalenyl)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 5-Amino-1-naphthol | HCID 65746 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Acetamide, N-(5-hydroxy-1-naphthalenyl)- | HCID 89653 | 84% |
반응 단계
Into a 500 ml round bottom flask (fitted with a magnetic stirrer), a 50:50 mixture of water:ethanol was combined with 5-amino-1-naphthol (20 g, 125 mmole) until the solid was completely dissolved. The solution was warmed to boiling and to it was added acetic anhydride (14 g) and the resulting solution was stirred for 1 hour. Upon cooling, crystals of N-(5-hydroxy1-napthyl)acetamide (21 g, 84% yield) formed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05372931 |
| 출처 데이터셋 | uspto-grants-1994_12 |
| ORD ID | ord-9841c85224a643b8b92313affe8bfdbc |
| 출처 메모 | uspto-grants-1994_12 |