Ammonia → HCID 15746509, 화합물

HRID 1492214노트

반응식

[CH3:1][C:2]1[C:7]([N:8]=[C:9]=[S:10])=[C:6]([N:11]2[CH2:16][CH2:15][O:14][CH2:13][CH2:12]2)[CH:5]=[CH:4][CH:3]=1.[NH3:17]>>[CH3:1][C:2]1[C:7]([NH:8][C:9]([NH2:17])=[S:10])=[C:6]([N:11]2[CH2:16][CH2:15][O:14][CH2:13][CH2:12]2)[CH:5]=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 222Ammonia

HCID 18952334HCID 18952334, 화합물

생성물 1

HCID 15746509HCID 15746509, 화합물

실험 절차

Reaction of 6-methyl-2-morpholinophenyl isothiocyanate (8.8 g) with 33% alcoholic ammonia solution (60 ml) at room temperature for 5 hours gave 1-(6-methyl-2-morpholinophenyl)thiourea (9 g) as a pale yellow solid, m.p. 199° C. which was recrystallised from a 1:1 mixture of ethylacetate and hexane.

출처 및 근거

ORD 기록: ord-40289cb7c4a2479ab0ab80be106aba0d
출처 데이터셋: uspto-grants-1994_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05373008

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