Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → 2-Methyl-3-(n-butyl)-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | 1-(n-Butyl)-3-(2-morpholinophenyl)thiourea | HCID 8625254 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 2-Methyl-3-(n-butyl)-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide | HCID 18952135 | — |
반응 단계
A mixture of 1-(n-butyl)-3-(2-morpholinophenyl)thiourea (5.8 g) and methyliodide (3.1 g) in acetone (25 ml) was heated at reflux for 4 hours to yield 2-methyl-3-(n-butyl)-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide as a colourless solid m.p. 154°-156° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05373008 |
| 출처 데이터셋 | uspto-grants-1994_12 |
| ORD ID | ord-ca5e95bd8be44316bca6fce21dc6827f |
| 출처 메모 | uspto-grants-1994_12 |