Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(Trifluoromethyl)phenol → 2,6-Di-(3-trifluoromethyl phenoxy)-4-methylthiopyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(Trifluoromethyl)phenol | HCID 7376 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 2,6-Dichloro-4-(methylthio)pyridine | HCID 18950231 | — |
| 생성물 | 2,6-Di-(3-trifluoromethyl phenoxy)-4-methylthiopyridine | HCID 21471060 | 85.3% |
반응 단계
A mixture of 2,6-dichloro-4-methylthiopyridine (0.97 g; 0.005 mol), 3-hydroxybenzotrifluoride (1.3 ml; 10.4 mmol) and sodium hydride (0.2 g) was reacted and worked up according to the procedure of Example 1 above to give 2,6-di-(3-trifluoromethyl phenoxy)-4-methylthiopyridine (1.9 g; 85%)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05374604 |
| 출처 데이터셋 | uspto-grants-1994_12 |
| ORD ID | ord-aa934b7d69004c628c57501ce6524b0d |
| 출처 메모 | uspto-grants-1994_12 |