Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Chloride → 1-Benzyl-1H-benzotriazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Chloride | HCID 7503 | — |
| 반응물 | HCID 178418385 | HCID 178418385 | — |
| 생성물 | 1-Benzyl-1H-benzotriazole | HCID 521212 | — |
| 생성물 | 2-Benzylbenzotriazole | HCID 3810549 | — |
반응 단계
(Phenylmethyl)-1H-benzotriazole was prepared from 1H-benzotriazole (11.91 g, 0.100 mol) and benzyl chloride as in Example 1 for 1 hour to give the title compound and (phenylmethyl)-2H- benzotriazole in a ratio of 75:25. Workup and two recrystallization gives the pure 1H-isomer: mp 117°-119° C. (CH3CN); (lit.1 mp 114°-117° C.; lit.2,3 mp 115°-116° C.)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05374701 |
| 출처 데이터셋 | uspto-grants-1994_12 |
| ORD ID | ord-8147f27b84604d19a1bee28ac32e0933 |
| 출처 메모 | uspto-grants-1994_12 |