참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetone, oxime | HCID 67180 | — |
| 반응물 | 4-{3-[4-(1-Chloroethyl)phenylthio]-5-fluorophenyl}-4-methoxytetrahydropyran | HCID 19379931 | — |
| 생성물 | HCID 9909885 | HCID 9909885 | 58% |
반응 단계
Using an analogous procedure to that described in Example 1 except that the reactants were heated to 60° C. for 2 hours, acetone oxime was reacted with 4-{3-[4-(1-chloroethyl)phenylthio]-5-fluorophenyl}-4-methoxytetrahydropyran to give acetone O-{4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)phenylthio)-α-methylbenzyl}oxime as an oil in 58% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05376680 |
|---|
| 출처 데이터셋 | uspto-grants-1994_12 |
|---|
| ORD ID | ord-eb32913a49604aa78cf550693e028e28 |
|---|
| 출처 메모 | uspto-grants-1994_12 |
|---|
