Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(oxan-4-ylidene)hydroxylamine → tetrahydropyran-4-one O-{4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)phenylthio]-alpha-methylbenzyl}oxime
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(oxan-4-ylidene)hydroxylamine | HCID 12298558 | — |
| 반응물 | 4-{3-[4-(1-Chloroethyl)phenylthio]-5-fluorophenyl}-4-methoxytetrahydropyran | HCID 19379931 | — |
| 생성물 | tetrahydropyran-4-one O-{4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)phenylthio]-alpha-methylbenzyl}oxime | HCID 19379937 | 74% |
반응 단계
Using an analogous procedure to that described in Example 1, tetrahydropyran-4-one oxime was reacted with 4-{3-[4-(1-chloroethyl)phenylthio]-5-fluorophenyl}-4-methoxytetrahydropyran to give tetrahydropyran-4-one O-{4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)phenylthio]-α-methylbenzyl}oxime as an oil in 74% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05376680 |
| 출처 데이터셋 | uspto-grants-1994_12 |
| ORD ID | ord-68ce202b88454e78bf074fbdfe5a1f4e |
| 출처 메모 | uspto-grants-1994_12 |