HCID 15143423, 화합물 → HCID 13685437, 화합물
반응식
C([O:8][CH2:9][C@H:10]([O:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])[CH3:11])C1C=CC=CC=1>[Pd].C(O)C>[CH2:13]([O:12][C@H:10]([CH3:11])[CH2:9][OH:8])[CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]참가 물질
4
실험 절차
A mixture liquid of the above (R)-1-benzyloxy-2-hexyloxy-propane (25 g),palladium/carbon catalyst (2.0 g) and ethanol (200 ml) was subjected to hydrogenolysis. After completion of the reaction, the catalyst was filtered off, followed by concentrating the mother liquor, and distilling the concentrate under reduced pressure to obtain (R)-2-hexyloxy-1-propanol (b.p. 67°-68° C./4 mmHg) (11.6 g).
후처리
- customAfter completion of the reaction
- filtrationthe catalyst was filtered off
- concentrationby concentrating the mother liquor
- distillationdistilling the
- concentrationconcentrate under reduced pressure
출처 및 근거
- ORD 기록
- ord-5d31cdb1a6644ed2a51519e74e855cb6
- 출처 데이터셋
- uspto-grants-1991_06
- 특허 번호
- US05021191
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