Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → N-[4-(4-t-butylphenoxy)-3-aminophenyl]methane sulphonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 4-tert-Butylphenol | HCID 7393 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | N-(4-chloro-3-nitrophenyl)methanesulfonamide | HCID 3755760 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 용매 | Diglyme | HCID 8150 | — |
| 생성물 | N-[4-(4-t-butylphenoxy)-3-aminophenyl]methane sulphonamide | HCID 19830594 | — |
반응 단계
N-(4-chloro-3-nitrophenyl)methanesulphonamide (50 g, 0.2 mole), 4-t-butylphenol (33 g, 0.22 mole), potassium carbonate (62.1 g, 0.45 mole) and diglyme (50 ml) were heated and stirred at 165°-170° for 24 hr. The mixture was cooled to 110° and xylene (150 ml) followed by a mixture of 10M-hydrochloric acid (55 ml) and water (130 ml) added.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05021333 |
| 출처 데이터셋 | uspto-grants-1991_06 |
| ORD ID | ord-ae428aa6bb0d4d399b66e410cbcd4fe2 |
| 출처 메모 | uspto-grants-1991_06 |