Methacrylic Acid → Copper(2+) bis(2-methylprop-2-enoate)

HRID 1493114노트

반응식

HRID 1493114 반응식
[O-]CC.[Cu+2:4].[O-]CC.[C:8]([OH:13])(=[O:12])[C:9]([CH3:11])=[CH2:10]>O1CCCC1>[C:8]([O-:13])(=[O:12])[C:9]([CH3:11])=[CH2:10].[Cu+2:4].[C:8]([O-:13])(=[O:12])[C:9]([CH3:11])=[CH2:10]

참가 물질

4

반응물 2

HCID 4093Methacrylic AcidHCID 14419876Ethanol, copper(2 ) salt

생성물 1

HCID 6452881Copper(2+) bis(2-methylprop-2-enoate)

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

1.50 Grams (0.009 mol) of copper (II) ethoxide was introduced into a 50 ml. round bottom flask having a magnetic spinning bar, in an argon atmosphere in a dry box. A solution of 1.84 g (0.02 mol) of methacrylic acid, prepared in 20 ml of anhydrous tetrahydrofuran was then added to it. The contents of the flask were agitated overnight (20 hr) by means of a magnetic stirrer at ambient temperature under argon. All volatile matter was then removed in vacuo (about 0.1 mm Hg) for 12 hours. The resulting solid was analyzed for its metal content.

후처리

  1. customround bottom flask having
  2. additionwas then added to it
  3. customAll volatile matter was then removed in vacuo (about 0.1 mm Hg) for 12 hours

출처 및 근거

ORD 기록
ord-7947042a76134bc88e2f125442b117f5
출처 데이터셋
uspto-grants-1991_06
특허 번호
US05021398

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