Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 5-(4-chlorophenyl)furan-2-carbonyl Chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 5-(4-Chlorophenyl)-2-furoic acid | HCID 726693 | — |
| 생성물 | 5-(4-chlorophenyl)furan-2-carbonyl Chloride | HCID 2771970 | — |
반응 단계
A mixture of 56 g. (0.25 mole) of 5-(p-chlorophenyl)-2-furoic acid and 100 ml. of SOCl2 is refluxed for 31/2 hours so that HCl gas evolves and there is dissolution. The SOCl2 is removed on a rotary evaporator. Benzene is added to the solid residue and is then removed on the rotary evaporator to give 5-(p-chlorophenyl)-2-furoyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05023272 |
| 출처 데이터셋 | uspto-grants-1991_06 |
| ORD ID | ord-df0a9281d2464af58cff782825a87b9e |
| 출처 메모 | uspto-grants-1991_06 |