Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonium Hydroxide → 5-(4-Chlorophenyl)furan-2-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 반응물 | 5-(4-chlorophenyl)furan-2-carbonyl Chloride | HCID 2771970 | — |
| 생성물 | 5-(4-Chlorophenyl)furan-2-carboxamide | HCID 4780001 | — |
반응 단계
To 1000 ml. of cold, stirring NH4OH, 63 g. (0.26 mole) of 5-(p-chlorophenyl)-2-furoyl chloride is added portionwise. The resulting mixture is stirred at ice bath temperature for 15 minutes and then is stored at room temperature for 18 hours. The solid is filtered, is washed with water and is dried at 60° to yield 56 g. (97%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05023272 |
| 출처 데이터셋 | uspto-grants-1991_06 |
| ORD ID | ord-2245ed9770494de7b665cb3ba76866c2 |
| 출처 메모 | uspto-grants-1991_06 |