Thionyl Chloride → HCID 53915754, 화합물

HRID 1494600노트

반응식

HRID 1494600 반응식
[CH:1]([C:3]1([C:12]([OH:14])=O)[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2].S(Cl)([Cl:17])=O>>[CH:1]([C:3]1([C:12]([Cl:17])=[O:14])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2]

참가 물질

3

반응물 2

HCID 24386Thionyl ChlorideHCID 19828700HCID 19828700, 화합물

생성물 1

HCID 53915754HCID 53915754, 화합물

실험 절차

A mixture 2,3-dihydro-2-vinyl-1H-indene-2-carboxylic acid (5.09 g) and thionyl chloride (25 ml) was refluxed for 10 hours. Excess thionyl chloride was distilled off under reduced pressure. The crude product was used as such for the following reaction.

후처리

  1. distillationExcess thionyl chloride was distilled off under reduced pressure
  2. customsuch for the following reaction

출처 및 근거

ORD 기록
ord-89f5ee2aa9fd40c395f9ef973cc3e60a
출처 데이터셋
uspto-grants-1991_06
특허 번호
US05026868

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