Sulfuric Acid → HCID 19828702, 화합물

HRID 1494601노트

반응식

HRID 1494601 반응식
[CH:1]([C:3]1([C:12](Cl)=[O:13])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2].[CH2:15](OC(=O)CC(O)=O)C.C(O[Mg])C.S(=O)(=O)(O)O>C(OCCCC)CCC>[CH:1]([C:3]1([C:12](=[O:13])[CH3:15])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2]

참가 물질

5

반응물 3

HCID 1118Sulfuric AcidHCID 53915754HCID 53915754, 화합물HCID 178472270HCID 178472270, 화합물

생성물 1

HCID 19828702HCID 19828702, 화합물

시약·촉매·용매 1

HCID 8909Butyl ether용매

실험 절차

1-(2,3-Dihydro-2-vinyl-1H-inden-2-yl)-ethanone was prepared by treating 2,3-dihydro-2-vinyl-1H-indene-2-carboxylic acid chloride with ethoxy magnesium malonic acid ethyl ester in dibutylether and after that with sulfuric acid according to the method of Reynolds, G.A. and Hauser, C.B., Org. Synth. 30 (1957) 70.

출처 및 근거

ORD 기록
ord-a1e39354742a419c82bb3d4aa17beda1
출처 데이터셋
uspto-grants-1991_06
특허 번호
US05026868

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