돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1494699생성일: 2026년 10월 25일

2-Amino-1-(2-mercapto-2-methylpropylamino)benzene → 1-[2-(trans-2-Butenylthio)-2-methylpropylamino]-2-(2-mercapto-2-methylpropylamino)benzene

https://huagongshe.com/reaction/1494699

반응식

참여 물질

역할이름HCID투입량
반응물2-Amino-1-(2-mercapto-2-methylpropylamino)benzeneHCID 10012927—
반응물2-(trans-2-Butenylthio)-2-methylpropanalHCID 10351953—
생성물1-[2-(trans-2-Butenylthio)-2-methylpropylamino]-2-(2-mercapto-2-methylpropylamino)benzeneHCID 1002004988.3%

반응 단계

2-Amino-1-(2-mercapto-2-methylpropylamino)benzene (0.36 g, 1.84×10-3 mol) and 0.58 g (3.67×10-3 mol, 200 M %) 2-(trans-2-butenylthio)-2-methylpropanal were reacted by the procedures in Example 2 to give 0.55 g (88% yield) 1-[2-(trans-2-butenylthio)-2-methylpropylamino]-2-(2-mercapto-2-methylpropylamino)benzene as an oil after purification by radial chromatography on a 4 mm silica plate eluting with 100% hexane.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05026913
출처 데이터셋uspto-grants-1991_06
ORD IDord-44e9e6a07a344ae680c5e5a44a2b4782
출처 메모uspto-grants-1991_06