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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1494707생성일: 2026년 10월 27일

2-(2-(Butylthio)2-methylpropylamino]-1-(2-mercapto-2-methylpropylamino)benzene → 2-Propanethiol, 1-anilino-2-methyl-

https://huagongshe.com/reaction/1494707

반응식

참여 물질

역할이름HCID투입량
반응물2-(2-(Butylthio)2-methylpropylamino]-1-(2-mercapto-2-methylpropylamino)benzeneHCID 10026859—
촉매Sodium pertechnetateHCID 74086836—
생성물2-Propanethiol, 1-anilino-2-methyl-HCID 143163—

반응 단계

2-(2-(Butylthio)2-methylpropylamino]-1-(2-mercapto-2-methylpropylamino)benzene was reacted with Tc-99m sodium pertechnetate by the method of Example 7 to produce Tc-99m complex of 2-(2-butylthio)2-methylpropylamino)-1-(2-mercapto-2-methylpropylamino)benzene. The complex was purified by filtration through Millex GS and Jelco 5 micron filters. HPLC (90% ethanol/H 2 O, 1.5 ml/min, C18 5 micron Radial Pak) Rt 4.4 min (99%). TLC (50% diethyl ether/chloroform) Rf 0.89, radiochemical purity 92%. Electrophoresis (0.05 M NaH2PO4, buffer pH 4.5 constant 300 volts, 30 min) neutral.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05026913
출처 데이터셋uspto-grants-1991_06
ORD IDord-30d7736693e04af7adb57249130b6cf8
출처 메모uspto-grants-1991_06